By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Kunihito KOUMOTO, Nagoya University, Japan Nicola ROMEO, University of Parma,
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Extra resources for 5th FORUM ON NEW MATERIALS PART C Proceedings of the 5th Forum on New Materials, part of CIMTEC 2010-12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 13-18, 2010
Mater. Submitted. jp Keywords: thermoelectric material, intermetallic compound, Heusler alloy, powder metallurgy. Abstract. Sb-doped Heusler Fe2VAl alloy was synthesized to evaluate the effect of heavy element doping on thermoelectric properties of the Heusler alloy. For the sample preparation, a pulse-current sintering technique with fine powder prepared by mechanical alloying was used. By using the powder metallurgy technique, a heavy element with a low melting point can be stably doped, compared to the melting process.
An important question is the positions of the Sr and Eu guest atoms in Ba8-xAxGa16Si30 (A=Sr, Eu; x=1, 2). The Rietveld structure refinements confirmed that the Sr and Eu guest atoms preferentially occupy the 28 5th FORUM ON NEW MATERIALS PART C 2a site in the smaller cage but the occupancy of Sr atoms on the 6d site is relatively large in comparison to Eu atoms. The similar trend was reported for Ba6Eu2Cu4Si42  and EuxBa8-xAl14Si31 . The structure refinements also show that the atomic displacement parameters ADPs on the 2a site for Ba8-xEuxGa16Si30 (x=1 and 2) are significantly increased by a factor more than two relative to Ba8Ga16Si30.
In this study, V site was substituted by Ti  to obtain the p-type Heusler alloy. 16), powders were prepared, yielding finely pulverized and homogenized particles. 9%) powders were mixed and milled in a planetary ball mill with a 500-ml-capacity Cr steel pot and balls. In the milling system, the pot rotates on its axis against the direction of orbital motion. The pot was back-filled with a purified Ar gas atmosphere at 500 Torr after creating a vacuum. A total mass of 400 g of 5-mm-diameter Cr steel balls was inserted with 30 g of mixed powder into the pot: MA was performed at 280 rpm for 5 h with a half hour rest every hour.